*1 Student, KVM Collage of pharmacy Cherthala, Alappuzha, Kerala, India.
2 Student, KVM Collage of pharmacy Cherthala, Alappuzha, Kerala, India.
3 Prof &HOD Department of pharmaceutics, KVM Collage of pharmacy Cherthala, Alappuzha, Kerala, India.
The aim of this research work is “Comparative study of formulated herbal face wash containing aloe vera with marketed preparation”. The face wash was prepared by using ingredients such as aloe vera, turmeric, neem, glycerine, honey, gelatine, vitamin E, methyl paraben, sodium lauryl sulphate and rose water. The face wash was prepared by homogenous mixing of all the excipients and the herbal extracts, therefore three formulation F1, F2 and F3 was prepared and evaluated. Several evaluation test such as organoleptic properties, homogeneity, pH, grittiness, microbial growth, viscosity, spreadability test, washability test, foamability test, test for irritancy and phase separation. The herbal face wash (F1&F2) showed good appearance, foam ability, washability, spreadability, pH, non-irritant and no phase separation was observed. Also, the herbal formulation shows no redness, itching and irritation during irritancy test and they were easily washable and stable at room temperature. The marketed preparation (F3) showed good appearance, foamability, microbial growth and no phase separation, but this preparation has shown burning sensation to the skin in irritancy test & difficult to wash off from skin. Therefore, formulation F3 was not optimised preparation. Based on the physio-chemical test, herbal formulation (F1) gave excellent result for all the parameters therefore, showing better stability and safety for skin products when compared to formulation F2 and F3. This suggests the potential effectiveness of herbal ingredients in skincare products.
Cosmetics are the products which are generally used to beautify the skin and also purify the skin. The word cosmetics is derived from Greek word – ?kosmesticos? which means to adorn. The materials that are used to promote appearances or to beautify the skin are called as cosmetics. From the ancient time till now people are still using poly herbal or herbal cosmetics for the beautification of skin. The use of herbal products as cosmetics is as prevalent in modern era as it was in ancient times. Herbal cosmetics are mostly preferred because it has less or nil side effects when compared to synthetic products and show enhanced effects upon application.[1]
Face skin is the major part of the body, which indicates the health of an individual It consists of materials such as amino acids, lipids and carbohydrates etc. So that a balanced nutrition is provided for the skin, that keeps it clear, glossy and healthy. It deals with the formulation and characterization of cosmetic ideal face wash preparation. In ancient times, conscious about their beauty and used to dress themselves because they wanted to increase their own beauty. Even today, people especially in rural areas, and hilly region select the natural remedies like plants extracts for cosmetics purposes like neem, aloe vera, turmeric, rose different clays to perform face washing and cleansing. Many cosmetics products are now available which are used to purify and beautify the skin. The main advantage for using these cosmetic washes and cleansing agents is that it is pure and does not have any side effects on the human body. Men have rough skin and when they don't take sufficient care then the skin turns dark due to over exposure to the sunlight which needs more attention in order to keep skin healthy and problems free.
Facial skin is delicate and ordinary soaps can cause moisture loss. A face wash is a mild cleanser that does the vital job of keeping skin clean, germ free, smooth fresh and moisturizes the horny layer without any harshness to the skin; helps look younger and energetic.
The purpose of facewash may be to impart cleansing, anti-wrinkle effect, anticancer property, moisturizing effect and fairness of skin.[2]
Face wash is highly beneficial in getting rid of dirt’s to the skin. All skin types have been proven to benefit equally from face wash products. Using a face wash every day is necessary and can help maintain healthy skin. The objectives of this work is to overcome the drawbacks of synthetic facewashes and to prepare herbal facewash so we made an attempt to formulate herbal face wash & topic is “Comparative study of formulated herbal contain aloe vera face wash with marketed preparation”
There are some important research articles that are being referred for this research work they are as follows;
The purpose of the present research work is
MATERIALS USED
Rose water
Rose water gives natural hydration to the skin. As the name rose water comes from the rich and fragrant petals of the rose flower. It has antioxidant properties and help to prevent wrinkles. Rose water proves to be effective in some of the major skin problems like dryness and breakouts.
Glycerine
Glycerine also improves skin function to slow down aging. It also traps moisture in your skin and gives a youthful, healthy glow. It provides anti-irritant protection to the skin. Glycerine accelerates wound healing.[5]
Methyl paraben
Methyl paraben is one of the most common parabens. It may be used in cosmetics as a preservative to protect against microbial (e.g. bacteria, fungus) growth. This gives product compatibility and product integrity. [6]
Sodium Lauryl Sulphate
In cosmetics, sodium Lauryl Sulphate is most often used as an emulsifier or surfactant. As an emulsifier, it helps to stabilize and thicken solutions with ingredients of differing solubility. This allows products to achieve a more uniform texture for easier, & smoother application. [7]
Figure 4: Sodium Lauryl Sulphate
Honey
Honey's natural humectant properties make it an effective moisturizer. it penetrates deeply into the skin and bring hydration to the underlying layers. This results in plumper, softer skin with a natural radiant glow. Honey is also an effective antimicrobial agent.
Gelatine
Gelatine is most commonly used as a gelling agent. It has moisture -retaining properties, providing deep hydration and help to revitalize the skin. Gelatine stimulates collagen production, promoting firmness and elasticity also gives a younger appearance.[8]
Vitamin E
Vitamin E containing face wash is gentle suitable for sensitive skin as it has soothing properties and helps to reverse the signs of skin aging. It also act as moisturizing agent, cleanser, it helps to lighten dark spots, relieve cold sores, stretch marks etc. [9]
Aloe vera
Aloe vera has many skin bene?ts, making our skin glow and soft. It is a magical plant that is used in such a large number of skin and hair care items. Apart from having medicinal properties, it has a lot of nourishing bene?ts as well. Aloe has an antioxidant property that prevents skin cell damage. It has a moisturizing effect on dry skin and help reduce irritation of skin.
Neem
Neem is a natural healer, so it can soothe and calm irritated skin. The antibacterial nature of neem leaves also prevents skin infections. Neem-containing face washes can help reduce redness and irritation while neem face pack gives a peaceful mind and also works effectively on blackheads and whiteheads. It has anti-aging properties that help in reducing wrinkles and fine lines.
Figure 9: Neem
Turmeric
Turmeric is an amazing ingredient for skin care. It can resolve a number of skin problems, including acne, skin darkening, skin pigmentation, rashes, infections etc. It has been used since ages to boost the health and glow of the skin.[10]
Methods Used For Obtaining Plant Extract
Mature, healthy and fresh aloe vera leaves were collected and washed with distilled water. Then after proper drying of leaves in hot air oven, the outer part of the leaves was dissected longitudinally using a sterile knife. Then the aloe vera gel that is the colourless parenchymatous tissue was removed using the sterile knife. Then it is filtrated using muslin cloth to remove the Fibers and impurities. Then the filtrate or the filter product which is a clear aloe vera gel was used in the preparation.[11]
Conventional extraction using Soxhlet: The rhizomes of turmeric were dried in oven at 105°c for 3 hours. Dried rhizomes were triturated using mortar and screened through a sieve with mesh 80 to obtain uniform powder with particle size of 0.18 mm. The turmeric powder was stored in refrigerator to prevent moisture uptake, the Soxhlet extraction, as the reference method, was pre-formed as follows: 15 g ground turmeric powder was weighed and embedded in a thimble and put in the Soxhlet apparatus which was gradually filled with acetone as the extraction solvent. The extraction experiment was carried out at 60°C within 8h. Upon completion of the extraction, the acetone was separated from the extract using rotary evaporator under vacuum at 35°C. The residue was dried and weighed. In all extraction experiments acetone was used as the extraction solvent due to its high solubilization capacity. [12]
The fully matured neem (azadirachta indica) leaves were collected and washed under distilled water within three times to remove complete dirt. Then the leaves were air dried for 10 days, then the dried leaves were collected and ground into a powder and stored into airtight bottles.[13]
Methods Used For Formulating Herbal Face Wash
Table 1: Composition Of Herbal Face Wash
Procedure
The double heat method is used for melting gelatine in face wash. 1gm of gelatine was taken & Aloe vera extract was added and mixed with continuous stirring to form aloe vera gel then the gel is used for F1&F2 preparations. F1 formulation contains aloe vera gel which was taken in a beaker. Then in this same beaker neem, honey, glycerine, vitamin E was added and mixed together with constant stirring. To this added few drops of rose water to give fragrance. F2 was also prepared in the same manner with addition turmeric instead of neem. F3 is a marketed preparation were marketed aloe vera gel, sodium lauryl sulphate, methyl paraben, honey, glycerine, vitamin E was added and mixed together. To this, added few drops of rose water as a fragrance. Then, final face wash was ready and packed in to the bottle.
Evaluation – Herbal Face Wash
Result And Discussion
Result are as follows,
F1 having neem and aloe vera the main ingredient that has moisturizing, anti- bacterial and anti- ageing property. F2 having ingredients like turmeric, aloe vera has anti-microbial and wound healing activity. F3 contains marketed aloe vera preparation. The organoleptic properties of formulated herbal face wash were evaluated and results was found to be satisfactory. Other physical parameters like homogeneity, pH, test for microbial growth, viscosity, foam ability, spreadability, wash ability, irritancy, phase separation, grittiness was also evaluated. The pH of the face wash was found to be 4.5-7.0 which is suitable for skin ph. The appearance and consistency of face wash was good.
Test for microbial growth i.e. zone of inhibition was performed and compared having formulations F1, F2 & F3. It was found that F3 is more effective than F1 & F2. Because F3 used as synthetic preservative i.e. methyl paraben. The viscosity of the face wash was performed, it is measured by using Ostwald viscometer. F1 & F2 are more stable than F3, due to it is good flow property & can be easily applied on to skin. Foamability test was performed and it was observed that F1&F2 have less forms compared to F3 due to synthetic foaming agent i.e. sodium lauryl sulphate. The spreadability test was also performed & it was observed that F1&F2 have more spreadability compared to formulation F3 when applied to the skin leads to poor patient compliance as it is difficult to get removed from skin. The wash ability of the face wash was performed, it was observed that formulation F1 &F2 were easily washable while F3 was not easily washable because formulation F3 contains high concentration of foaming agent like Sodium lauryl Sulphate.
Irritancy test was performed F1&F2 are non-irritant and F3 shows irritation like burning sensation when applied to the skin. The phase separation was conducted for 24 hours for 20 days, there was no signs of phase separation that indicates all the formulations F1, F2& F3 are stable because they contain highly rich antioxidant property of aloe vera, turmeric & neem. F3 added as synthetic preservative like methyl paraben. Hence, this comparative study of herbal face wash with marketed preparation revealed that herbal formulation (F1) gave excellent result for all the parameters therefore, showing better stability and safety for skin products when compared to formulation F2 and F3.
From this research work it can be concluded that herbal skin care products are natural products that will stimulate moisturizing, anti-aging, anti-inflammatory, anti-microbial, antioxidant and wound healing activity. This herbal skin care product has fewer side effect and no irritation when compared with synthetic ones.
CONCLUSION
It is a successful attempt to create herbal face wash with a variety of plants that have therapeutic advantages. Herbal formulation has growing demand in the world market. It is a very good effort to establish an herbal facial wash, which includes aloe vera, turmeric, neem. Herbal face washes are used to refresh the muscles, keep the skin elastic, get rid of stuck-on grime, and enhance blood ?ow. The face wash gives the skin the necessary nutrition. It aids in the removal of scars, marks, and pimples. Skin is exfoliated by facewashes, which also have a cooling, soothing, and soothing impact on the skin. They do so in the quickest possible time of bring back the skin’s natural radiance. Regular usage of natural face wash enhances appearance and texture to skin. The impact of pollution and harsh conditions on the skin can be mitigated by using face wash on a regular basis. They aid in keeping skin cells elastic and prevent the skin from ageing too quickly. Natural face can be used to successfully control wrinkles, ?ne lines, and skin loosening. We discovered outstanding qualities in the face wash in our study, but more research is required to determine its full potential as a cosmetic. Natural medicines are now widely recognised since they are less likely to have negative effects than products with a chemical base and are safer. To meet the demands of the expanding global market, numerous herbal formulations are needed. It is a successful attempt to create an herbal face wash with a variety of plants that have therapeutic advantages.
In this study, it was found that the formulated herbal face wash was found to be safe, effective, non-toxic and improves patient compliance. It believes that natural remedies are more acceptable and safer with fewer side effects than the synthetic ones.
REFERENCES
Athulya Lal, Nimisha Mathew, Dr. Lincy John, Comparative Study Of Formulated Herbal Face Wash With Marketed Preparation, Int. J. of Pharm. Sci., 2024, Vol 2, Issue 6, 480-487. https://doi.org/10.5281/zenodo.11543092